Table of Contents
Purpose
This test is done by sieving through a 600 micron sieve for the determination of residues of bituminous emulsions.
Device
- 600 micron sieve A circular sieve of about 100 mm in diameter and 40 mm in height.
- metal or glass dish – A small metal or glass vessel (such as a watch glass) of about 110 mm in diameter.
- Oven – A well ventilated oven thermostatically controlled from 100 to 110″C.
- Remanent – A capacity 250g and accuracy 0.01g and a capacity 10kg and accuracy 1g.
- Pot – A clean, weighed, 1.5-liter container.
Process
- Wash the 600 µm IS sieve with xylene and then with acetone. Place it in the dish, in the oven at 100 . dry on0C to 1100C for one hour, refrigerate and, with dish, weigh down to the nearest 0.01 g (W.)1,
- Remove the sieve from the sieve and moisten with the solution. Remove the 4-liter sample by stirring it slowly and immediately strain it through a sieve into a clean, dry-weight container (W.)4,
- room temperature and 50 . Filter the emulsion at low and high viscosity0c respectively. When the entire emulsion is drained through the sieve, remove the sieve and weigh the container to the nearest 1 g (W.)2,
- Wash the strainer repeatedly with distilled water until the wash runs clear. Put the sieve in a small pot in the oven for two hours at 105±5. keep to dry0C. Cool and weigh together to the nearest 0.01 g (W.)3,
Calculate the residuals as follows:
Residue, Percentage Retained = (W.)3 – woo1) / (w2 – woo4) x 100
Where
woo1 = mass of sieve and small vessel in g
woo2 = mass in g of container and emulsion
woo3 = mass of the strainer, small plate and residue in g; And
woo4 = mass of container in g
Take the average of the three values obtained for the residuals, percentage.
requirement criteria
type of bituminous emulsion | Residue on 600 µm IS Sieve |
Rapid Setting-1 (RS-1) | 0.05 |
Rapid Setting-2 (RS-2) | 0.05 |
medium setting (ms) | 0.05 |
Slow Setting -1 (SS-1) | 0.05 |
Slow Setting-2 (SS-2) | 0.05 |
Reference
IS 8887 – 2004
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